at 10E-4-10E-5 Torr, high excess of aromatics, react. container at -196°C, inlets for organic educts heated to let them as vapor. Cr vaporized at ca 1600-1800°C for 60-80 min.; filtrn., evapn. till beginnig of sublimation, solved in benzene, chromy.(Kieselgel, benzene:diethylether=40:1), elem. anal.;
sodium hydroxide; E. coli penicillin-G acylase F24A mutant T=25°C; pH=9.4; Title compound not separated from byproducts;
参考文献
Carboni, Chiara; Kierkels, Hans G. T.; Gardossi, Lucia; Tamiola, Kamil; Janssen, Dick B.; Quaedflieg, Peter J. L. M.
Tetrahedron Asymmetry, 2006 , vol. 17, # 2 p. 245 - 251