4,4'-二甲氧基二苯安合成路线 （共 60 条）
反应条件
boron tribromide in dichloromethane
参考文献
Ohta, Kiminori; Chiba, Yuki; Ogawa, Takumi; Endo, Yasuyuki
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 5050 - 5053
反应条件
potassium hydroxide; water; tetra-(n-butyl)ammonium iodide
1.) benzene, 88 deg C, 1 h, 2.) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Dinnocenzo, J. P.; Banach, T. E.
Journal of the American Chemical Society, 1989 , vol. 111, # 23 p. 8646 - 8653
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Ohta, Kiminori; Chiba, Yuki; Ogawa, Takumi; Endo, Yasuyuki
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 5050 - 5053
参考文献
Kainer; Hausser
Chemische Berichte, 1953 , vol. 86, p. 1563,1566
反应条件
hydrogenchloride; ethanol; water; sodium nitrite
参考文献
Koshechko, V. G.; Inozemtsev, A. N.; Pokhodenko, V. D.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 4 p. 662 - 666
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 4 p. 751 - 756
反应条件
1: sodium tert-butoxide; tri-tert-butylphosphine / Pd2(dba)3 / toluene / 7 h / 100 °C
2: 2.755 g / aq. NaOH / ethanol / 1 h / Heating
View Scheme
参考文献
Murata, Hidenori; Lahti, Paul M.
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4974 - 4977
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate; dipalladiumtris(benzylideneacetone) in toluene
T=110°C; 15 h;
参考文献
Barlow, Stephen; Risko, Chad; Chung, Sung-Jae; Tucker, Neil M.; Coropceanu, Veaceslav; Jones, Simon C.; Levi, Zerubba; Bredas, Jean-Luc; Marder, Seth R.
Journal of the American Chemical Society, 2005 , vol. 127, # 48 p. 16900 - 16911
反应条件
tris-(o-tolyl)phosphine; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
Substitution;
参考文献
Michinobu, Tsuyoshi; Tsuchida, Eishun; Nishide, Hiroyuki
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 4 p. 1021 - 1027
反应条件
copper; potassium carbonate in nitrobenzene
Substitution; Ullmann reaction; Heating;
参考文献
Shimada, Tomoyuki; Sasaki, Masaomi; Aruga, Tamotsu; Umeda, Minoru
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 4 p. 785 - 793
反应条件
T=-20°C; dann beim Aufloesen Chloroform;
参考文献
Wieland; Wecker
Chemische Berichte, 1910 , vol. 43, p. 708
