反应条件
n-butyllithium in tetrahydrofuran Ar atmosphere; addn. of n-BuLi to diphenyl ether in THF (0°C), addn. of B(OMe)3 (0°C), stirring (room temp., 1 h); pouring into aq. HCl, extn. (ether), drying of ether layer (over Na2SO4), evapn., column chromy. (silica gel, EtOAc/hexane 1:3), recrystn. ether/hexane); elem. anal.;
参考文献
Ishihara, Kazuaki; Maruyama, Tohru; Mouri, Makoto; Gao, Qingzhi; Furuta,Kyoji; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 11 p. 3483 - 3491
