in neat (no solvent)
byproducts: Br2, FNO; Irradiation (UV/VIS); irradiated for 12 h with λmax = 420 nm; condensed into a cylinder held at -196°C, vac. transferred into another cylinder, condensed several times (trap-to-trap); obtained with apurity of ca 98percent;
参考文献
Lu, Norman; Thrasher, Joseph S.; Von Ahsen, Stefan; Willner, Helge; Hnyk, Drahomir; Oberhammer, Heinz
Inorganic Chemistry, 2006 , vol. 45, # 4 p. 1783 - 1788
Arden, E. A.; Phillips, L.; Shaw, R.
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Gray, P.; Shaw, R.; Thynne, J. C. J.
Progr. Reaction Kinetics, 1967 , vol. 4, p. 63 - 117
