1-(喹啉-2-基)乙酮合成路线 (共 46 条)
反应条件
sodium hydride; xylene
参考文献
Boekelheide; Weinstock
Journal of the American Chemical Society, 1952 , vol. 74, p. 660,663
反应条件
in benzene
0.5 h; Ambient temperature;
参考文献
Yamamoto; Ouchi; Tanaka
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 6 p. 1028 - 1030
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in water
T=60°C;
参考文献
Citterio, Attilio; Gentile, Anna; Serravalle, Marco; Tinucci, Laura; Vismara, Elena
Journal of Chemical Research, Miniprint, 1982 , # 10 p. 2801 - 2815
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in water
T=50°C; 7 h;
参考文献
Citterio, Attilio; Gentile, Anna; Serravalle, Marco; Tinucci, Laura; Vismara, Elena
Journal of Chemical Research, Miniprint, 1982 , # 10 p. 2801 - 2815
反应条件
aminosulfonic acid in tetrahydrofuran
Inert atmosphereReflux;
参考文献
Mroczek, Agnieszka; Erre, Giulia; Taras, Rossana; Gladiali, Serafino
Tetrahedron Asymmetry, 2010 , vol. 21, # 15 p. 1921 - 1927
反应条件
toluene
und Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure bis auf 105grad;
参考文献
Campbell et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1844
反应条件
N,N,N',N'-tetramethylguanidine in toluene
T=110°C; 0.5 h; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Nomland, Ashley; Hills, Ivory D.
Tetrahedron Letters, 2008 , vol. 49, # 38 p. 5511 - 5514
反应条件
tert.-butylhydroperoxide; iron nitrate (III) in pyridine; acetic acid
T=60°C; Yield given. Yields of byproduct given;
参考文献
Minisci, Francesco; Fontana, Francesca; Bravo, Anna; Yan, Yong Ming
Gazzetta Chimica Italiana, 1996 , vol. 126, # 2 p. 85 - 88
反应条件
tert.-butylhydroperoxide; iron nitrate (III) in pyridine; acetic acid
T=20°C; 18 h; Yield given. Yields of byproduct given;
参考文献
Minisci, Francesco; Fontana, Francesca; Bravo, Anna; Yan, Yong Ming
Gazzetta Chimica Italiana, 1996 , vol. 126, # 2 p. 85 - 88
反应条件
bromine; sodium acetate; acetic acid
und Erhitzen des Reaktionsgemisches mit wss. Schwefelsaeure;
参考文献
Brown
Journal of the Chemical Society, 1949 , p. 2577