N1-环己基-4-(1-哌啶甲基)-1,2-苯二胺合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated carbon in ethanol P=760.051 Torr; 1 h;
参考文献
Biogen Idec Ma Inc.
Patent: US2011/152260 A1, 2011 ;
Location in patent: Page/Page column 10 ;
反应条件
1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / -10 - 0 °C 1.2: Chromatography 2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.12 h / 130 °C / Microwave irradiation 3.1: hydrogen / palladium on activated carbon / ethanol / 1 h / 760.05 Torr View Scheme
参考文献
Biogen Idec Ma Inc.
Patent: US2011/152260 A1, 2011 ;
反应条件
1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / -10 - 0 °C 1.2: Chromatography 2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.12 h / 130 °C / Microwave irradiation 3.1: hydrogen / palladium on activated carbon / ethanol / 1 h / 760.05 Torr View Scheme
参考文献
Biogen Idec Ma Inc.
Patent: US2011/152260 A1, 2011 ;
