(甲氧基-苯基甲基)苯合成路线 (共 143 条)
反应条件
1: (S)-2-(3,4-Dimethoxy-phenyl)-8-(1,3-diphenyl-propyl)-5,7-dimethoxy-chroman With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile
T=20°C; Oxidation; 2 h;
2: diphenyldiazo-methane in tetrahydrofuran; methanol
T=20°C; Alkylation; 19.1 h; Further byproducts given;
参考文献
Kozikowski, Alan P.; Tueckmantel, Werner; George, Clifford
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5371 - 5381
参考文献
Bergmann; Hervey
Chemische Berichte, 1929 , vol. 62, p. 915
反应条件
para-dicyanobenzene in acetonitrile
T=15°C; 2 h; Irradiation;
参考文献
Tomioka, Hideo; Inoue, Osamu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1404 - 1406
反应条件
T=60°C; electrooxidation;
参考文献
Parker, Vernon D.; Bethell, Donald
Journal of the American Chemical Society, 1987 , vol. 109, # 17 p. 5066 - 5072
反应条件
para-dicyanobenzene in methanol; acetonitrile
T=80°C; 18 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Okamoto, Akio; Snow, Miles S.; Arnold, Donald R.
Tetrahedron, 1986 , vol. 42, # 22 p. 6175 - 6187
参考文献
Ramsden, Christopher A.; Rose, Helen L.
Synlett, 1997 , vol. 1997, # 1 p. 27 - 28
反应条件
iron (III) perchlorate
3 h; Heating;
参考文献
Salehi, Peyman; Irandoost, Mohsen; Seddighi, Behnam; Kargar Behbahani, Farahnaz; Tahmasebi, Daryush Poor
Synthetic Communications, 2000 , vol. 30, # 10 p. 1743 - 1747
反应条件
triethylsilane; Nafion-H (perfluororesinsulfonic acid) in dichloromethane
4 h; Heating;
参考文献
Olah, George A.; Yamato, Takehiko; Iyer, Pradeep; Prakash, G.K. Surya
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2826 - 2828
反应条件
in benzene
0.5 h; Ambient temperature;
参考文献
Ishikawa, Hiroshi; Mukaiyama, Teruaki; Ikeda, Shigeru
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 776 - 780
反应条件
in methanol
7 h; Heating;
参考文献
Popielarz; Arnold
Journal of the American Chemical Society, 1990 , vol. 112, # 8 p. 3068 - 3082