3,4,5-三甲氧基异氰酸苯酯合成路线 （共 11 条）
反应条件
sodium azide in water; acetone 1 h;
参考文献
Belin, Florence; Barthelemy, Philippe; Ruiz, Karine; Lacombe, Jean Michel; Pucci, Bernard
Helvetica Chimica Acta, 2003 , vol. 86, # 2 p. 247 - 265
反应条件
in toluene 6 h; Heating;
参考文献
European Journal of Medicinal Chemistry, , vol. 33, # 11 p. 839 - 858
反应条件
diphenylphosphoranyl azide; triethylamine in toluene T=65°C; 2.5 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 32, # 5 p. 377 - 384
反应条件
1.) CH3Ph/ether, reflux, 1.5 h; 2.) CH3Ph, 1.5 h;
参考文献
Brown; Moudachirou
Tetrahedron, 1994 , vol. 50, # 34 p. 10309 - 10320
反应条件
in toluene T=100°C; Cooling with ice;
参考文献
European Journal of Medicinal Chemistry, , vol. 44, # 8 p. 3318 - 3322
反应条件
1: potassium hydroxide / ethanol; water / 3 h / Reflux 2: thionyl chloride / 21 h / 80 °C 3: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / water; acetone; toluene / 10 - 15 °C 4: 80 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 85, # 2 p. 236 - 244
参考文献
Schloegl,K.; Schloegl,R.
Monatshefte fuer Chemie, 1964 , vol. 95, p. 942 - 949
参考文献
Jin, Yi; Zhou, Zu-Yu; Tian, Wei; Yu, Qiang; Long, Ya-Qiu
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 22 p. 5864 - 5869
参考文献
Metabio-Joullie
Patent: US4252804 A1, 1981 ;
