反应条件
in n-heptane; toluene
(strict exclusion of air and moisture), Fe complex in toluene cooled to -15°C, treated dropwise wit 2 equiv. of Me2AlCl in heptane, stirred at -15°C for 1 h, treated with pyridine at 0°C, warmed at room temp. for 20 h (stirring); centrifuged, evapd., washed (pentane), dissolved (toluene), treated withpuridine, stirred for 2 h, centrifuged, evapd.(vac.), washed (pentane), elem. anal.;
参考文献
Wrackmeyer, Bernd; Klimkina, Elena V.; Milius, Wolfgang
European Journal of Inorganic Chemistry, 2009 , # 21 p. 3155 - 3162
