3,5-二叔丁基邻苯二酚合成路线 (共 187 条)
反应条件
oxygen in tetrahydrofuran; water
T=25°C; P=760.051 Torr; 68 h;
参考文献
Sartorel, Andrea; Carraro, Mauro; Scorrano, Gianfranco; Bassil, Bassem S.; Dickman, Michael H.; Keita, Bineta; Nadjo, Louis; Kortz, Ulrich; Bonchio, Marcella
Chemistry - A European Journal, 2009 , vol. 15, # 32 p. 7854 - 7858
反应条件
1: With 1-(2-pyridylmethyl)pyrrolidine-2-carboxylic acid; oxygen; triethylamine in acetonitrile
T=20°C; 12.0333 h;
2: With hydrogenchloride in water
参考文献
Paria, Sayantan; Halder, Partha; Paine, Tapan Kanti
Inorganic Chemistry, 2010 , vol. 49, # 10 p. 4518 - 4523
反应条件
1: With C19H25Cl3FeN5O; sodium tetraphenyl borate; triethylamine in acetonitrile
3652.5 h; Inert atmosphere;
2: With oxygen in acetonitrile
6 h;
参考文献
Wagner, Marit; Limberg, Christian; Tietz, Thomas
Chemistry - A European Journal, 2009 , vol. 15, # 22 p. 5567 - 5576
反应条件
dihydrogen peroxide; organic copolymer linked metallophthalocyanine in phosphate buffer; acetonitrile
T=20°C; pH=7; Product distribution; Further Variations:CatalystsSolventsReagentspH-values;
参考文献
Sanchez, Muriel; Chap, Nicolas; Cazaux, Jean-Bernard; Meunier, Bernard
European Journal of Inorganic Chemistry, 2001 , # 7 p. 1775 - 1783
反应条件
oxygen; FeCl(DTBC)py2 in tetrahydrofuran; pyridine
T=25°C; P=760 Torr; 24 h; var. of catalyst, catechol, conc.; Product distribution;
参考文献
Funabiki, Takuzo; Ishikawa, Michiya; Nagai, Yasutaka; Yorita, Jun; Yoshida, Satohiro
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1951 - 1952
反应条件
silver perchlorate monohydrate; [Fe((2-methoxyethyl)bis(1-methyl-1H-imidazol-2-ylmethyl)amine)Cl3]; oxygen; triethylamine
T=25°C; 4 h;
参考文献
Sundaravel, Karuppasamy; Suresh, Eringathodi; Saminathan, Kolandaivel; Palaniandavar, Mallayan
Dalton Transactions, 2011 , vol. 40, # 32 p. 8092 - 8107
反应条件
ClFe(2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol-2H); oxygen in N,N-dimethyl-formamide
48.25 h; Sealed tube; Reagent/catalyst;
参考文献
Farrell, Joshua R.; Niconchuk, Jonathan A.; Renehan, Peter R.; Higham, Christine S.; Yoon, Eric; Andrews, Mark V.; Shaw, Janet L.; Cetin, Anil; Engle, James; Ziegler, Christopher J.
Dalton Transactions, 2014 , vol. 43, # 18 p. 6610 - 6613
反应条件
pyridine; oxygen; iron(II) chloride in tetrahydrofuran
T=25°C; P=760 Torr; also FeCl3, also H2O at var conc.; Product distributionMechanism;
参考文献
Funabiki, Takuzo; Yoneda, Izumi; Ishikawa, Michiya; Ujiie, Mikio; Nagai, Yasutaka; Yoshida, Satohiro
Journal of the Chemical Society, Chemical Communications, 1994 , # 12 p. 1453 - 1454
反应条件
in dichloromethane
(N2), quenched with N2 to stop further oxidation; extn. with water, evapn. at reduced pressure, extn. with n-pentane, chromatographed on a silica gel column, NMR;
参考文献
Bianchini, Claudio; Frediani, Piero; Laschi, Franco; Meli, Andrea; Vizza, Francesco; Zanello, Piero
Inorganic Chemistry, 1990 , vol. 29, p. 3402 - 3409
反应条件
C13H17Cl2FeN4O; oxygen in methanol
T=25°C; 12 h; Kinetics; Reagent/catalyst;
参考文献
Sundaravel, Karuppasamy; Sankaralingam, Muniyandi; Suresh, Eringathodi; Palaniandavar, Mallayan
Dalton Transactions, 2011 , vol. 40, # 33 p. 8444 - 8458