0.00416667 h;

lithium hydroxide hydrate; Pd/DNA in water T=80°C; 20 h; Inert atmosphere;

1: With ytterbium; methyl iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 2 h; 2: With 1-naphthaldehyde in tetrahydrofuran 2 h; Heating; Further stages.;

1.1: sodium tetrahydroborate / methanol / 1 h / |Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / |Inert atmosphere 2.2: 1 h / 0 °C / |Inert atmosphere 2.3: 2 h / 0 - 20 °C / |Inert atmosphere View Scheme