3-反-溴碳-2,2'-二甲基氧酸酯合成路线 （共 39 条）
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid in dichloromethane T=0°C; 0.5 h;
参考文献
Belanger, Dominique; Tong, Xia; Soumare, Sadia; Dory, Yves L.; Zhao, Yue
Chemistry - A European Journal, 2009 , vol. 15, # 17 p. 4428 - 4436
反应条件
triethylsilane; palladium 10 on activated carbon in acetone T=20°C; 0.5 h; Inert atmosphere;
参考文献
Trajkovic, Milos; Ferjancic, Zorana; Saicic, Radomir N.
Tetrahedron Asymmetry, 2012 , vol. 23, # 8 p. 602 - 604
反应条件
diisobutylaluminium hydride T=-78°C;
参考文献
Yin, Jianming; Liu, Hanlan; Pidgeon, Charles
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 2 p. 179 - 182
反应条件
lithium aluminium tetrahydride in diethyl ether T=5°C; 1.5 h;
参考文献
Bold, Guido; Allmendinger, Thomas; Herold, Peter; Moesch, Luzia; Schaer, Hans-Peter; et al.
Helvetica Chimica Acta, 1992 , vol. 75, # 3 p. 865 - 882
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran; dimethyl sulfoxide 0.416667 h; Ambient temperature;
参考文献
Bose, D. Subhas; Srinivas
Synlett, 1998 , # 9 p. 977 - 978
反应条件
bis[(S,S,S)-DiazaPhos-SPE] in tetrahydrofuran T=55°C; P=7240.26 Torr; 72 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Clemens, Alexander J. L.; Burke, Steven D.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2983 - 2985
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 355 - 359
反应条件
1: K2CO3 / dimethylformamide / 0 - 20 °C 2: 90.7 percent / TsOH / Heating 3: 90.4 percent / DIBALH / -78 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 8, # 2 p. 179 - 182
反应条件
diisobutylaluminium hydride T=-78°C;
参考文献
Coelho, Fernando; Diaz, Gaspar; Abella, Carlos A. M.; Almeida, Wanda P.
Synlett, 2006 , # 3 p. 435 - 439
反应条件
1: 1.) SOCl2, 2.) Et3N / 1.) RT, reflux, 8 h, 2.) CH2Cl2, RT, 8 h 2: TsOH*H2O / benzene / Heating 3: NaBH4, LiCl / ethanol; tetrahydrofuran / 4 h / Ambient temperature 4: 1.) trifluoroacetic anhydride, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 1 h, 2.) CH2Cl2, from -78 deg C to 25 deg C View Scheme
参考文献
Tetrahedron, , vol. 52, # 36 p. 11673 - 11694
