2-甲基-3-氧代-2-丁烷基乙酸酯合成路线 （共 19 条）
反应条件
sulfuric acid; mercuric sulphate
参考文献
Bergmann; Herman
Journal of Applied Chemistry, 1953 , vol. 3, p. 42,48
反应条件
1: diluted HCl 2: concentrated H2SO4 / zuletzt auf dem Wasserbad View Scheme
参考文献
Nasarow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1940 , p. 219
Chem.Abstr., 1942 , p. 746
反应条件
in ethylene glycol dimethyl ether; acetic acid
参考文献
Thorpe,J.W.; Warkentin,J.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 927 - 935
参考文献
Gillis,B.T.; Hagarty,J.D.
Journal of Organic Chemistry, 1967 , vol. 32, p. 95 - 96
参考文献
Crandall,J.K. et al.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1149 - 1154
参考文献
Singh, Megh; Murray, Robert W.
Journal of Organic Chemistry, 1992 , vol. 57, # 15 p. 4263 - 4270
参考文献
Thorpe,J.W.; Warkentin,J.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 927 - 935
参考文献
McMahon et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2976
反应条件
1.1: BF3*Et2O / CH2Cl2 / 0.5 h / -40 - 0 °C
1.2: 100 percent / N,N-diisopropylethylamine / CH2Cl2 / 1 h / -78 - 20 °C
2.1: NaOMe / ethanol / 8 h / Heating
View Scheme
参考文献
Jensen, Mark S.; Hoerrner, R. Scott; Li, Wenjie; Nelson, Dorian P.; Javadi, Gary J.; Dormer, Peter G.; Cai, Dongwei; Larsen, Robert D.
Journal of Organic Chemistry, 2005 , vol. 70, # 15 p. 6034 - 6039
