2-(2-溴丙-2-烯基)苯甲酰胺合成路线 (共 4 条)
反应条件
sodium hydroxide in water T=20°C; 2 h;
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 553 - 557
反应条件
potassium carbonate in dimethyl sulfoxide T=110°C; 24 h;
参考文献
Yasmin, Nasima; Ray, Jayanta K.
Synlett, 2009 , # 17 p. 2825 - 2827
反应条件
1: 1.) phenyl-lithium, 2.) lithium naphthalenide / 1.) diethyl ether, THF, -78 deg C, 30 min, 2.) -78 deg C, 2 h
2: 91 percent / H2O / diethyl ether; tetrahydrofuran / Ambient temperature; reactions with other electrophiles
View Scheme
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 553 - 557
反应条件
1: NaH / dimethylformamide
2: 30 percent / Bu3SnH; AIBN / benzene / Heating
View Scheme
参考文献
Palframan, Matthew J.; Tchabanenko, Kirill; Robertson, Jeremy
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8423 - 8425