(9H-芴-9-基)甲基 2,5-二氧代吡咯烷-1-羧酸合成路线 (共 36 条)
反应条件
sodium carbonate in 1,4-dioxane
参考文献
Song, Yan-Li; Roller, Peter P.; Long, Ya-Qiu
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 12 p. 3205 - 3208
反应条件
sodium carbonate in 1,4-dioxane 18 h; Ambient temperature; Yield given;
参考文献
Crivici; Lajoie
Synthetic Communications, 1993 , vol. 23, # 1 p. 49 - 53
反应条件
sodium carbonate; toluene-4-sulfonic acid 1) dioxane, gas pressure: 350 mbar, 3 d, r.t., 2) dioxane, 0 deg C to r.t., 14 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lajoie; Crivici; Adamson
Synthesis, 1990 , # 7 p. 571 - 572
反应条件
acetic acid in ethanol pH=8;
参考文献
Seitz, Oliver; Koehler, Olaf
Chemistry - A European Journal, 2001 , vol. 7, # 18 p. 3911 - 3925
反应条件
potassium carbonate in 1,4-dioxane T=20°C;
参考文献
MAX-PLANCK-GESELLSCHAFT ZUR FÖRDERUNG DER WISSENSCHAFTEN E.V.; GOPALAKRISHNAN, Ranganath; HAUSCH, Felix
Patent: WO2013/91900 A1, 2013 ;
Location in patent: Page/Page column 41 ;
反应条件
potassium carbonate in 1,4-dioxane T=20°C;
参考文献
MAX-PLANCK-GESELLSCHAFT ZUR FÖRDERUNG DER WISSENSCHAFTEN E.V.; GOPALAKRISHNAN, Ranganath; HAUSCH, Felix
Patent: WO2013/91900 A1, 2013 ;
Location in patent: Page/Page column 41 ;
反应条件
sodium carbonate; toluene-4-sulfonic acid 1) dioxane, gas pressure: 350 mbar, 3 d, r.t., 2) dioxane, 0 deg C to r.t., 14 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lajoie; Crivici; Adamson
Synthesis, 1990 , # 7 p. 571 - 572
反应条件
hydrogen; sodium hydrogencarbonate; palladium on activated charcoal 1) ethanol, overnight; 2) dioxane, ice-bath, 70 min; Yield given. Multistep reaction;
参考文献
Marsh, Ian R.; Bradley, Mark; Teague, Simon J.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6199 - 6203
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=20°C;
参考文献
Vernall, Andrea J.; Stoddart, Leigh A.; Briddon, Stephen J.; Ng, Hui Wen; Laughton, Charles A.; Doughty, Stephen W.; Hill, Stephen J.; Kellam, Barrie
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5673 - 5682
反应条件
sodium hydrogencarbonate in water; acetone T=20°C; 1 h;
参考文献
Hossany, B. Rehana; Johnston, Blair D.; Wen, Xin; Borrelli, Silvia; Yuan, Yue; Johnson, Margaret A.; Pinto, B. Mario
Carbohydrate Research, 2009 , vol. 344, # 12 p. 1412 - 1427