N-(2,6-二氯苯基)苯甲酰胺合成路线 （共 15 条）
反应条件
bis(trimethylaluminum)-1,4-diazabicyclo[2.2.2]octane in tetrahydrofuran T=130°C; 0.133333 h; Inert atmosphereMicrowave irradiation;
参考文献
Dubois, Nathalie; Glynn, Daniel; McInally, Thomas; Rhodes, Barrie; Woodward, Simon; Irvine, Derek J.; Dodds, Chris
Tetrahedron, 2013 , vol. 69, # 46 p. 9890 - 9897
反应条件
thionyl chloride in diethyl ether 1 h; T < 5 deg C;
参考文献
Ayyangar, Nagaraj R.; Kalkote, Uttam R.; Nikrad, Pandurang V.
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1099 - 1102
反应条件
boron trifluoride in dichloromethane T=-78°C; 4 h;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
boron trifluoride in dichloromethane T=25°C;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
boron trifluoride in dichloromethane T=-78°C; 6 h;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
in dichloromethane T=20°C;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
in dichloromethane T=-50°C;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
1: HBF4 / hexane; diethyl ether / -50 °C 2: 10 percent / CH2Cl2 / -50 °C View Scheme
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
in dichloromethane T=-50°C; Further byproducts given;
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
1: NaHCO3 / diethyl ether; H2O / 1 h / T < 5 deg C; or in benzene 2: 77 percent / SOCl2 / diethyl ether / 1 h / T < 5 deg C View Scheme
参考文献
Ayyangar, N. R.; Kalkote, U. R.; Nikrad, P. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 872 - 877
