in not given
formation of PH3*BBr3 by react. of PH3 with BBr3 at 25 °C; decompn. of PH3*BBr3 on heating at 300 °C;; formation of amorphous PB;;
参考文献
Vickery, R. C.
Nature (London, United Kingdom), 1959 , vol. 184, p. 268
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Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 113, p. 78 - 80
in neat (no solvent)
using N2 as a carrier gas; heating at 473 - 493 K using the hot tube method according to: C.A. Brown and A. W. Laubengayer, J. Am. Chem. Soc. 77, 3699 (1955);
参考文献
Kazakov; Timoshkin
Russian Journal of Inorganic Chemistry, 2012 , vol. 57, # 4 p. 557 - 563
in benzene-d6
under N2 or Ar, BBr3 and C6D6 distd. into NMR tube contg. Rh complex, sealed off under vac., reacted for 6 h; not isolated; analyzed by NMR;
参考文献
Zheng, Limin; Baker, R. Thomas; Knobler, Carolyn B.; Walker, John A.; Hawthorne, M. Frederick
Inorganic Chemistry, 1983 , vol. 22, p. 3350 - 3355
