Abel, E. W.; Gerrard, W.; Lappert, M. F.
Journal of the Chemical Society, 1957 , p. 5051 - 5054
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Gmelin Handbook: B: B-Verb.9, 6.2.4, page 286 - 292
byproducts: boron hydride, benzene, C3H8; High Pressure; under N2; diborane and trihalogen-borane was added to cumene at -130°C, then in a closed autoclave the mixture was heated to 130°C for 90 min; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed, unseparable isomers; elem. anal.;
methyloxirane in dichloromethane (N2); treatment of germanium compd. with propilene oxide and boron compd. in CH2Cl2 at -78°C and then with pinacol room temp.;
参考文献
Turner, David J.; Anemian, Remi; MacKie, Philip R.; Cupertino, Domenico C.; Yeates, Stephen G.; Turner, Michael L.; Spivey, Alan C.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 11 p. 1752 - 1763
Behrend, P.
Journal fuer Praktische Chemie (Leipzig), 1877 , vol. 15, p. 23 - 42
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Gustavson, G.
Ber., 1873 , vol. 6, p. 9 - 11
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Gmelin Handbook: S: MVol.B3, 131, page 1807 - 1808