in neat (no solvent) vapour of MoO3 condensed and then reacted with excess of vapour of BCl3 at -196°C in vac.; heated to 20°C in vac., heated to 100°C;
参考文献
Cook, Neil D.; Timms, Peter L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 239 - 244
MoO3 is reacted with BCl3 to several products; MoCl6 is not produced;
参考文献
Brisdon, Alan K.; Graham, John T.; Hope, Eric G.; Jenkins, Delyth M.; Levason, William; Ogden, J. Steven
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , # 5 p. 1529 - 1532
Burch, J. E.; Gerrard, W.; Howarth, M.; Mooney, E. F.
Journal of the Chemical Society, 1960 , p. 4916 - 4918
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.4.4, page 157 - 159
