1: With [CpFe(CO)2(PCy3)][BF4]; phenyl silane T=100°C; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 10 p. 1879 - 1884
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 54, # 8 p. 1777 - 1779
