1: With [CpFe(CO)2(PCy3)][BF4]; phenyl silane T=100°C; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 10 p. 1879 - 1884
triethyl borane in hexane; benzene addn. of hexane soln. of Et3B to a soln. of methyl cinnamate and Bu3SnH in benzene at 25°C under Ar, stirring for 15 h at 25°C; concn. in vac., chromy. on silica gel (hexane/ethyl acetate);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 8 p. 2585 - 2587
RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
