1: Pd(OAc)2 / diethyl ether; CH2Cl2 / 1.5 h / -10 °C 2: 2 M aq. NaOH / methanol / 2 h / Ambient temperature 3: diphenyl phosphorazidate, triethylamine / 42 h / 90 °C 4: 1 M aq. HCl / 100 °C View Scheme
参考文献
Vallgarda; Appelberg; Arvidsson; Hjorth; Svensson; Hacksell
Journal of Medicinal Chemistry, 1996 , vol. 39, # 7 p. 1485 - 1493
aluminium trichloride in nitrobenzene T=70 - 75°C; 12 h;
参考文献
Balayan, R. S.; Akopyan, M. G.; Vartanyan, R. M.; Kaltrikyan, A. A.; Avakyan, O. M.; et al.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 8 p. 558 - 562
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 8 p. 956 - 960
