potassium hydroxide; hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane T=50°C; var. temp.: 20 deg C; add. of tricaprylmethylammonium chloride or polyethyleneglycol monomethylether; var. solv.: Et2O or n-pentane; add of m- and p-chloropropylbenzene: competitive reduction; Rate constant;
in benzene-d6 react. of Fe complex and HSiMe3 in benzene, 90°C, 9 h; yields detd. by (1)H-NMR (C5H5Fe(CO)H(SiMe3)2; elem. anal.) and GL-chromy. (other products);
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1790 - 1792