in diethyl ether a suspn. of complex in diethyl ether was treated with an ether soln. of Li-anilide at -78°C, warmed to room temp. (Ar); filtered, the solvent was removed under reduced pressure, not sepd., detected by NMR spectra;
tris-(2-chloro-ethyl)-amine; sulfuric acid in chloroform T=0°C; 0.0833333 h; other dialkyl acylphosphonates; var. temperature; var. time; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 116, # 3 p. 1016 - 1026
