Rezende, Michelle J. C.; Pereira, Mirian S. C.; Santos, Gabriel F. N.; Aroeira, Gabriel O. P.; Albuquerque Jr., Tiago C.; Suarez, Paulo A. Z.; Pinto, Angelo C.
Journal of the Brazilian Chemical Society, 2012 , vol. 23, # 7 p. 1209 - 1215
triethylamine in acetonitrile
0.333333 h; Ambient temperature;
参考文献
Vijayaraghavan, S. T.; Balasubramanian, T. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 760 - 761
1: With isopropylmagnesium chloride in tetrahydrofuran
T=25 - 40°C; 1.5 h; Inert atmosphereSchlenk technique;
2: With sulfuric acid in tetrahydrofuran; water
Cooling with ice;
