（s）-2,3-二羟基丙酸甲酯合成路线 （共 16 条）
反应条件
hydrogenchloride; methanol 1 h; Ambient temperature;
参考文献
Bhatia, Suresh K.; Hajdu, Joseph
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 5034 - 5039
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran T=0 - 20°C; 24 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=20°C; 24 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
1: MEP With water; (S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc in tetrahydrofuran T=0 - 20°C; 24 h; 2: N-Boc-2-nitrobenzenesulfonamide in tetrahydrofuran T=20°C; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 30 p. 3952 - 3954
反应条件
H(1+) form ion exchange resin in methanol T=60°C; 5 h;
参考文献
Hirth; Walther
Helvetica Chimica Acta, 1985 , vol. 68, # 7 p. 1863 - 1871
反应条件
1: (L)-serine With sulfuric acid; sodium nitrite 2: trimethyl orthoformate With sulfuric acid in methanol
参考文献
Sakoh, Hiroki; Sakuraba, Shunji; Sugimoto, Yuichi; Imamura, Hideaki; Jona, Hideki; Yamada, Koji; Bamba-Nagano, Rie; Hashizume, Terutaka; Morishima, Hajime
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 1 p. 163 - 165
参考文献
Fernandez, Carlos; Gandara, Zoila; Gomez, Generosa; Covelo, Berta; Fall, Yagamare
Tetrahedron Letters, 2007 , vol. 48, # 16 p. 2939 - 2942
反应条件
methanol; bromine 1.5 h; Heating;
参考文献
Barros; Maycock; Thomassigny
Synlett, 2001 , # 7 p. 1146 - 1148
反应条件
toluene-4-sulfonic acid in methanol 18 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 68, # 7 p. 1863 - 1871
