1-甲基-2-[(E)-2-(2-甲基苯基)乙烯基]苯合成路线 (共 19 条)
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); water; urea in 1-methyl-pyrrolidin-2-one T=20 - 130°C; P=3750.38 Torr; 15 h; AutoclaveInert atmosphere;
参考文献
Huang, Qiufeng; Hua, Ruimao
Chemistry - A European Journal, 2009 , vol. 15, # 15 p. 3817 - 3822
参考文献
Lawrence, Nicholas J.; Muhammad, Faiz
Tetrahedron Letters, 1994 , vol. 35, # 32 p. 5903 - 5906
参考文献
Aitken, R. Alan; Hodgson, Philip K. G.; Oyewale, Adebayo O.; Morrison, John J.
Chemical Communications, 1997 , # 13 p. 1163 - 1164
反应条件
titanium tetrachloride; zinc in tetrahydrofuran McMurry reaction; 4 h; Reflux;
参考文献
Rauniyar, Vivek; Zhai, Huimin; Hall, Dennis G.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8481 - 8490
反应条件
dirhodium tetraacetate in tetrahydrofuran T=-20 - 0°C; 0.166667 h; cis/trans ratio 11.9; Yield given;
参考文献
Shankar, B.K. Ravi; Shechter, Harold
Tetrahedron Letters, 1982 , vol. 23, # 22 p. 2277 - 2280
反应条件
ammonia; sodium amide in acetonitrile
参考文献
Jones,G.C.; Hauser,C.R.
Journal of Organic Chemistry, 1962 , vol. 27, p. 806 - 814
反应条件
(i) nBuLi, (ii) (thermolysis); Multistep reaction;
参考文献
Bookham, Jonathan L.; Smithies, Darren M.; Wright, Anna; Thornton-Pett, Mark; McFarlane, William
Journal of the Chemical Society - Dalton Transactions, 1998 , # 5 p. 811 - 818
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
参考文献
Chess, Edward K.; Lin, Ping-Huang; Gross, Michael L.
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1522 - 1527
反应条件
carbon dioxide; sulfur T=200 - 205°C;
参考文献
Szperl
Roczniki Chemii, vol. 6, p. 731,732
Chem. Zentralbl., 1927 , vol. 98, # I p. 2985
反应条件
(i) nBuLi, (ii) air; Multistep reaction;
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 26 p. 7417 - 7426