1-甲基-2-[(E)-2-(2-甲基苯基)乙烯基]苯合成路线 (共 19 条)
反应条件
1: various solvent(s) / Heating 2: aq. sodium hydroxide / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Bookham, Jonathan L.; Smithies, Darren M.; Wright, Anna; Thornton-Pett, Mark; McFarlane, William
Journal of the Chemical Society - Dalton Transactions, 1998 , # 5 p. 811 - 818
反应条件
sodium hydroxide in dichloromethane 0.5 h; Ambient temperature;
参考文献
Bookham, Jonathan L.; Smithies, Darren M.; Wright, Anna; Thornton-Pett, Mark; McFarlane, William
Journal of the Chemical Society - Dalton Transactions, 1998 , # 5 p. 811 - 818
反应条件
T=120 - 130°C; Behandeln des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Spaeth
Monatshefte fuer Chemie, 1914 , vol. 35, p. 466
参考文献
Szperl
Roczniki Chemii, 1926 , vol. 6, p. 736
反应条件
bei der elektrolytischen Reduktion;
参考文献
Law
Journal of the Chemical Society, 1907 , vol. 91, p. 759
反应条件
propylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) irradiation, 18 h, 2.) benzene, reflux, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lapouyade, Rene; Veyres, Alain; Hanafi, Naima; Couture, Axel; Lablache-Combier, Alain
Journal of Organic Chemistry, 1982 , vol. 47, # 7 p. 1361 - 1364
反应条件
air; iodine in cyclohexane 11 h; Irradiation;
参考文献
Rubin, Mordecai B.; Welner, Samuel
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1847 - 1852
反应条件
propylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) irradiation, 18 h, 2.) benzene, reflux, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lapouyade, Rene; Veyres, Alain; Hanafi, Naima; Couture, Axel; Lablache-Combier, Alain
Journal of Organic Chemistry, 1982 , vol. 47, # 7 p. 1361 - 1364
反应条件
1: bromine / CCl4 / 0.5 h / 70 °C
2: potassium hydroxide / ethanol / 12 h / Heating
View Scheme
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 26 p. 7417 - 7426