3,4,5,6,7,8-六氢-2(1H)-喹啉酮合成路线 (共 16 条)
反应条件
in 1,4-dioxane
3 h; Heating; Yield given;
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
sodium hydride; benzene
参考文献
Elad; Ginsburg
Journal of the Chemical Society, 1953 , p. 4137
反应条件
Erhitzen ueber den Schmelzpunkt;
参考文献
Lions
Journal and Proceedings of the Royal Society of New South Wales, 1937 , vol. 71, p. 192,206
反应条件
lithium aluminium tetrahydride in diethyl ether
1 h;
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
1: 79 percent / LAH / diethyl ether / 1 h
2: 90 percent / Et3N / diethyl ether / 0.5 h / Ambient temperature
View Scheme
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
lithium aluminium tetrahydride
1.) ether, 0 deg C, then RT, 3 h, 2.) -15 deg C; Yield given. Multistep reaction;
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412