反应条件
in tetrahydrofuran byproducts: tBu3SiH, tBu3SiBr, (tBu3Si)2; equimolar ratio, stirring (-78°C, 12 h), warming (room temp.); volatile compds. removal (vac.), dissoln. (pentane), filtn., pptn. (1 week, -23°C); elem. anal.;
参考文献
Wiberg, Nils; Amelunxen, Kerstin; Noeth, Heinrich; Schmidt, Martin; Schwenk, Holger
Angewandte Chemie (International Edition in English), 1996 , vol. 35, # 1 p. 65 - 67