4-哌啶-1-基-苯甲醛合成路线 （共 12 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide 20 h; Reflux;
参考文献
Russian Journal of General Chemistry, , vol. 83, # 10 p. 1864 - 1868
Zh. Obshch. Khim., , vol. 83, # 10 p. 1654 - 1659,6
反应条件
sulfuric acid; trifluoroacetic acid T=20°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 25 p. 8747 - 8757
反应条件
1: 49 percent / BINAP; t-BuOK / Pd2(dba)3 / toluene / 5 h / 80 °C 2: 73 percent / aq. H2SO4; trifluoroacetic acid / 2 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 25 p. 8747 - 8757
反应条件
1: 49 percent / BINAP; t-BuOK / Pd2(dba)3 / toluene / 5 h / 80 °C 2: 73 percent / aq. H2SO4; trifluoroacetic acid / 2 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 25 p. 8747 - 8757
反应条件
aluminum oxide 0.0208333 h; microwave irradiation;
参考文献
Synthetic Communications, , vol. 30, # 24 p. 4479 - 4488
参考文献
Organic Preparations and Procedures International, , vol. 30, # 4 p. 455 - 460
反应条件
in dimethyl sulfoxide 13 h; HeatingIrradiation;
参考文献
Tetrahedron Letters, , vol. 39, # 17 p. 2471 - 2474
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.75 h; Inert atmosphere; optical yield given as percent de;
参考文献
Duan, Xin-Fang; Feng, Jian-Xia; Zi, Guo-Fu; Zhang, Zhan-Bin
Synthesis, 2009 , # 2 p. 277 - 282
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.75 h; Inert atmosphere; optical yield given as percent de;
参考文献
Duan, Xin-Fang; Feng, Jian-Xia; Zi, Guo-Fu; Zhang, Zhan-Bin
Synthesis, 2009 , # 2 p. 277 - 282
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.75 h; Inert atmosphere; optical yield given as percent de;
参考文献
Duan, Xin-Fang; Feng, Jian-Xia; Zi, Guo-Fu; Zhang, Zhan-Bin
Synthesis, 2009 , # 2 p. 277 - 282
