N,N-二乙基 2-氟苯甲酰胺合成路线 （共 5 条）
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
反应条件
sec-BuLi in tetrahydrofuran; cyclohexane
参考文献
Air Products and Chemicals, Inc.
Patent: US5233074 A1, 1993 ;
反应条件
1: oxalyl chloride / DMF / CH2Cl2 / 2.5 h 2: CH2Cl2 / 16 h View Scheme
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
反应条件
N,N,N',N,-tetramethylethylenediamine; Davis reagent; sec.-butyllithium 1) THF, cyclohexane, -78 deg C, 1 h, 2) to room temperature, 12 h; Yield given. Multistep reaction;
参考文献
De Silva; Reed; Billedeau; Wang; Norris; Snieckus
Tetrahedron, 1992 , vol. 48, # 23 p. 4863 - 4878
反应条件
zirconocene dichloride; lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=20°C; 0.0333333 h; Inert atmosphere;
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
