对硝基苯-Alpha-D-吡喃甘露糖苷合成路线 （共 18 条）
反应条件
mutant malA D320G from Sulfolobus solfataricus in N,N-dimethyl-formamide T=20°C; pH=7; 96 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Yamamoto, Keisuke; Davis, Benjamin G.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 30 p. 7449 - 7453
反应条件
6(A),6(D)-di-C-cyano(hydroxy)methyl-β-cyclodextrin; water T=59°C; pH=8; 6 h; aq. phosphate buffer; Kinetics; Reagent/catalystConcentration; chemoselective reaction;
参考文献
Bjerre, Jeannette; Bols, Mikael
European Journal of Organic Chemistry, 2010 , # 18 p. 3487 - 3500
反应条件
mutant malA D320G from Sulfolobus solfataricus in N,N-dimethyl-formamide T=20°C; pH=7; 96 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Yamamoto, Keisuke; Davis, Benjamin G.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 30 p. 7449 - 7453
反应条件
α-D-galactosidase; sodium salt of phosphorous acid in N,N-dimethyl-formamide
参考文献
Nilsson, Kurt G. I.
Carbohydrate Research, 1987 , vol. 167, p. 95 - 104
反应条件
1: pyridine / 24 h 2: pyridine / 5 h / Ambient temperature 3: 80percent aq. AcOH / 20 h / Ambient temperature 4: 68 percent / 3-nitro-1-(2,4,6-triisopropylbenzenesulfonyl)-1,2,4-triazole / pyridine / 18 h / 37 °C / var. reag.: DCC 5: 83 percent / Et3N, MeOH, H2O / 16 h / 4 °C View Scheme
参考文献
Srivastava, Om. P.; Hindsgaul, Ole
Carbohydrate Research, 1985 , vol. 143, p. 77 - 84
反应条件
1: pyridine / 24 h 2: pyridine / 5 h / Ambient temperature 3: 80percent aq. AcOH / 20 h / Ambient temperature 4: 68 percent / 3-nitro-1-(2,4,6-triisopropylbenzenesulfonyl)-1,2,4-triazole / pyridine / 18 h / 37 °C / var. reag.: DCC 5: 83 percent / Et3N, MeOH, H2O / 16 h / 4 °C View Scheme
参考文献
Srivastava, Om. P.; Hindsgaul, Ole
Carbohydrate Research, 1985 , vol. 143, p. 77 - 84
反应条件
mutant malA D320G from Sulfolobus solfataricus in N,N-dimethyl-formamide T=20°C; pH=7; 96 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Yamamoto, Keisuke; Davis, Benjamin G.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 30 p. 7449 - 7453
反应条件
Jack bean α-mannosidase; methyl α-D-mannoseptanoside
pH=4.5; 0.333333 h; aq. bufferEnzymatic reaction; Kinetics; Reagent/catalyst;
参考文献
Boone, Matthew A.; Mcdonald, Frank E.; Lichter, Joseph; Lutz, Stefan; Cao, Rui; Hardcastle, Kenneth I.
Organic Letters, 2009 , vol. 11, # 4 p. 851 - 854
