(9Z)-9-十六碳烯-1-醇合成路线 （共 46 条）
反应条件
1: (i) O3, CH2Cl2, (ii) Ph3P
2: (i) K, HMPT, (ii) /BRN= 1769551/
3: aq. NaOH / methanol
View Scheme
参考文献
Bestmann; Stransky; Vostrowsky; Range
Chemische Berichte, 1975 , vol. 108, # 11 p. 3582 - 3595
反应条件
2: (i) O3, CH2Cl2, (ii) Ph3P
3: (i) K, HMPT, (ii) /BRN= 1769551/
4: aq. NaOH / methanol
View Scheme
参考文献
Bestmann; Stransky; Vostrowsky; Range
Chemische Berichte, 1975 , vol. 108, # 11 p. 3582 - 3595
反应条件
1: boron trifluoride diethyl etherate
2: potassium carbonate / toluene / 4 h / |Reflux
3: lithium aluminium tetrahydride / diethyl ether / 2 h / |Reflux
View Scheme
参考文献
Majee
Journal of the Indian Chemical Society, 2012 , vol. 89, # 10 p. 1435 - 1438
反应条件
sodium hydride; dimethyl sulfoxide in tetrahydrofuran
0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
pyridine
1 h; Ambient temperature;
参考文献
Chattopadhyay, S.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 236 - 237
参考文献
Baumann,W.J.; Mangold,H.K.
Journal of Organic Chemistry, 1964 , vol. 29, p. 3055 - 3057
