9,10-二(氯甲基)蒽合成路线 (共 18 条)
反应条件
hydrogenchloride in acetic acid T=60°C; 20 h;
参考文献
Bag, Bamaprasad; Bharadwaj, Parimal K.
Journal of Physical Chemistry B, 2005 , vol. 109, # 10 p. 4377 - 4390
反应条件
dichloromethane Substitution; dimerization; laser-jet photolysis; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 14 p. 3280 - 3287
参考文献
Journal of the Chemical Society, , p. 802,805
US1910462 , ;
DE533850 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 585,586
反应条件
in toluene 6 h; Heating;
参考文献
Wunz; Dorr; Alberts; Tunget; Einspahr; Milton; Remers
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1313 - 1321
反应条件
1.1: Na / o-xylene / 0.33 h / 100 °C 1.2: 56 percent / xylene / 4 h / Heating 2.1: 100 percent / aq. NaOH / H2O; ethanol / 2 h View Scheme
参考文献
Postowskii; Bednjagina
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 2919,2923
Chem. Zentralbl., 1938 , vol. 109, # II p. 3920
反应条件
potassium carbonate in toluene 24 h; Heating;
参考文献
Bissell, Richard A.; Calle, Emilio; Silva, A. Prasanna de; Silva, Saliya A. de; Gunaratne, H. Q. Nimal; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 9 p. 1559 - 1564
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Heating;
参考文献
Keck, Gary E.; Webb, Robert R.; Yates, John B.
Tetrahedron, 1981 , vol. 37, # 23 p. 4007 - 4016
反应条件
sodium bromide in acetone
参考文献
Clements, John H.; Webber
Macromolecules, 2004 , vol. 37, # 4 p. 1531 - 1536
参考文献
Seo, Bo Min; Seo, Ji Hoon; Kim, Jun Ho; Park, Jung Sun; Lee, Kum-Hee; Park, Min Hye; Yoon, Seung Soo; Kim, Young Kwan
Molecular Crystals and Liquid Crystals, 2011 , vol. 550, p. 233 - 239
参考文献
Liu, Wei; Wang, Yalong; Sun, Mingxiao; Zhang, Deteng; Zheng, Meng; Yang, Wenjun
Chemical Communications, 2013 , vol. 49, # 54 p. 6042 - 6044