1.1: iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride / tetrahydrofuran / 0.25 h / -20 °C 1.2: 16 h / -20 - 20 °C 2.1: LiH3BNMe2 / tetrahydrofuran / 16 h / -20 - 20 °C View Scheme
参考文献
Chemical Communications, , vol. 48, # 10 p. 1580 - 1582
1: With trans-N,N′-bis(2-pyridinylmethylene)-1,2-cyclohexanediamine; iron(II) chloride in tetrahydrofuran T=-78°C; 0.25 h; 2: With NaBEt3H in tetrahydrofuran T=-78 - 20°C; 16 h;
参考文献
Chemical Communications, , vol. 48, # 10 p. 1580 - 1582
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, # 3 p. 620 - 622
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 679 - 681
