1,3-bis-(diphenylphosphino)propane; acetic acid; triethylamine; palladium dichloride T=120°C; P=7600.51 Torr; 3 h; Autoclave;

sodium formate; palladium diacetate; N-ethyl-N,N-diisopropylamine; lithium chloride in N,N-dimethyl-formamide T=20°C; 0.833333 h;

sodium formate; palladium diacetate; N-ethyl-N,N-diisopropylamine; lithium chloride in N,N-dimethyl-formamide T=20°C;

1: phosphorus tribromide 2: sodium chlorite; dihydrogen peroxide 3: palladium dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; acetic acid / 3 h / 120 °C / 7600.51 Torr / |Autoclave View Scheme