N,O-双三甲硅基乙酰胺合成路线 （共 163 条）
反应条件
methanol
1.) 35-40 deg C, 2 h, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Gonda, Josef; Antalova, Zuzana
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 685 - 694
反应条件
triethylamine; paraformaldehyde in dichloromethane; water
参考文献
Monsanto Company
Patent: US4740608 A1, 1988 ;
反应条件
N,N'-bis(2-pyridylmethyl)-(1R,2R)-cyclohexane-1,2-diamine; molybdenum hexacarbonate in tetrahydrofuran
Alkylation; 0.0833333 h; microwave irradiation; Product distribution; Further Variations:SolventsTemperaturesirradiation power and reaction time;
参考文献
Kaiser, Nils Fredrik K.; Bremberg, Ulf; Larhed, Mats; Moberg, Christina; Hallberg, Anders
Angewandte Chemie - International Edition, 2000 , vol. 39, # 20 p. 3596 - 3598
反应条件
triethylamine in chloroform
参考文献
Bollmark; Stawinski
Chemical Communications, 2001 , # 8 p. 771 - 772
反应条件
in chloroform-d1
T=20°C; 0.25 h;
参考文献
Nemoto, Tetsuhiro; Masuda, Takamasa; Matsumoto, Takayoshi; Hamada, Yasumasa
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7172 - 7178
参考文献
Kantlehner,W. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 512 - 527
反应条件
in acetonitrile
T=20°C;
参考文献
Semaine, Wassila; Johar, Monika; Tyrrell, D. Lorne J.; Kumar, Rakesh; Agrawal
Journal of Medicinal Chemistry, 2006 , vol. 49, # 6 p. 2049 - 2054
参考文献
Heathcock, Clayton H.; Buse, Charles T.; Kleschick, William A.; Pirrung, Michael C.; Sohn, John E.; Lampe, John
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1066 - 1081
参考文献
Young, Robert J.; Shaw-Ponter, Sue; Hardy, George W.; Mills, Gail
Tetrahedron Letters, 1994 , vol. 35, # 46 p. 8687 - 8690
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
