N,O-双三甲硅基乙酰胺合成路线 (共 163 条)
反应条件
methanol
1.) 24 h; Yield given. Multistep reaction;
参考文献
Gonda, Josef; Antalova, Zuzana
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 685 - 694
反应条件
tin(IV) chloride
1.) CH2Cl2, RT, 3 h, 2.) CH2Cl2, RT, overnight; Yield given. Multistep reaction;
参考文献
Rosowsky; Kim; Wick
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1177 - 1181
反应条件
tin(IV) chloride
1.) CH2Cl2, RT, overnight, 2.) CH2Cl2, 25 deg C, overnight; Yield given. Multistep reaction;
参考文献
Rosowsky; Kim; Wick
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1177 - 1181
参考文献
White,E. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4241 - 4244
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
in tetrachloromethane
参考文献
Krauss, Dietlinde; Mainx, Hans Georg; Tauscher, Bernhard; Bischof, Peter
Organic Mass Spectrometry, 1985 , vol. 20, # 10 p. 614 - 618
反应条件
in tetrachloromethane
参考文献
Krauss, Dietlinde; Mainx, Hans Georg; Tauscher, Bernhard; Bischof, Peter
Organic Mass Spectrometry, 1985 , vol. 20, # 10 p. 614 - 618
反应条件
in tetrachloromethane
参考文献
Krauss, Dietlinde; Mainx, Hans Georg; Tauscher, Bernhard; Bischof, Peter
Organic Mass Spectrometry, 1985 , vol. 20, # 10 p. 614 - 618
反应条件
in acetonitrile
Ambient temperature;
参考文献
Mann, John; Tench, Allen J.; Weymouth-Wilson, Alexander C.; Shaw-Ponter, Sue; Young, Robert J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 6 p. 677 - 682
反应条件
tetrabutylammomium bromide
T=105°C; 4 h; Title compound not separated from byproducts.;
参考文献
Smietana, Michael; Mioskowski, Charles
Organic Letters, 2001 , vol. 3, # 7 p. 1037 - 1039