二乙基(2-乙基氯)磷酸盐合成路线 （共 11 条）
反应条件
T=190°C; Michaelis-Arbuzov reaction; 2 h; Microwave irradiationNeat (no solvent);
参考文献
USTAV ORGANICKE CHEMIE A BIOCHEMIE AKADEMIE VED CESKE REPUBLIKY, v.v.i.; JANSA, Petr; HOLY, Antonin; CESNEK, Michal
Patent: WO2012/13168 A1, 2012 ;
Location in patent: Page/Page column 22-23 ;
反应条件
T=140°C; 24 h; Inert atmosphereNeat (no solvent);
参考文献
Fourgeaud, Pierre; Midrier, Camille; Vors, Jean-Pierre; Volle, Jean-Noel; Pirat, Jean-Luc; Virieux, David
Tetrahedron, 2010 , vol. 66, # 3 p. 758 - 764
反应条件
pyridine; diethyl ether
参考文献
Bliznyuk,N.K. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, p. 1119 - 1122,1061 - 1063
反应条件
T=190°C; Michaelis-Arbuzov reaction; 2 h; Microwave irradiationNeat (no solvent);
参考文献
Jansa, Petr; Holy, Antonin; Dracinsky, Martin; Baszczynski, Ondrej; Cesnek, Michal; Janeba, Zlatko
Green Chemistry, 2011 , vol. 13, # 4 p. 882 - 888
反应条件
T=175 - 180°C; Isomerisierung;
参考文献
Kabatschnik; Rossiskaja
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 99
Chem.Abstr., 1948 , p. 5846
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene 1 h; Heating;
参考文献
Balczewski, Piotr; Pietrzykowski, Witold M.
Tetrahedron, 1996 , vol. 52, # 43 p. 13681 - 13694
参考文献
Ginsburg; Jakubowitsch
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 728,732; engl.Ausg.S.710,712,713
反应条件
potassium hydroxide in ethanol Inert atmosphereCoolingReflux;
参考文献
Fourgeaud, Pierre; Midrier, Camille; Vors, Jean-Pierre; Volle, Jean-Noel; Pirat, Jean-Luc; Virieux, David
Tetrahedron, 2010 , vol. 66, # 3 p. 758 - 764
反应条件
hydrogenchloride T=110°C; 12 h; atmospheric pressure;
参考文献
Revue Roumaine de Chimie, , vol. 49, # 6 p. 501 - 506
