4-甲氧基-2-(1-苯乙基)-苯酚合成路线 (共 8 条)
反应条件
iron/aluminium-doped nanoporous KIT-5 silica (FeAl-KIT-5) catalyst in cyclohexane 4 h; Reflux;
参考文献
Varghese, Shaji; Nagarajan, Samuthira; Benzigar, Mercy R.; Mano, Ajayan; Alothman, Zeid A.; Raj, George Allen Gnana; Vinu, Ajayan
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1485 - 1489
反应条件
cyclopentene in toluene T=100°C; 8 h; Inert atmosphere; regioselective reaction;
参考文献
Lee, Dong-Hwan; Kwon, Ki-Hyeok; Yi, Chae S.
Journal of the American Chemical Society, 2012 , vol. 134, # 17 p. 7325 - 7328
反应条件
iron(III) chloride in dichloromethane T=50°C; Friedel-Crafts alkylation; 20 h;
参考文献
Iovel, Irina; Mertins, Kristin; Kischel, Jette; Zapf, Alexander; Beller, Matthias
Angewandte Chemie - International Edition, 2005 , vol. 44, # 25 p. 3913 - 3917
反应条件
iron(III) chloride in cyclohexane T=80°C; 20 h;
参考文献
Chu, Cheng-Ming; Huang, Wan-Ju; Liu, Ju-Tsung; Yao, Ching-Fa
Tetrahedron Letters, 2007 , vol. 48, # 39 p. 6881 - 6885
反应条件
bismuth trifluoromethanesulphonate in dichloromethane T=55°C; Friedel-Crafts-type benzylation; 8 h;
参考文献
Rueping, Magnus; Nachtsheim, Boris J.; Ieawsuwan, Winai
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1033 - 1037
反应条件
oligomeric (4-methoxyphenoxy)alumoxane
参考文献
Inoyatov, F. Kh.; Abubakirov, R. Sh.; Mikaya, A. I.; Khrapova, I. M.; Perchenko, V. M.; Plate, N. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 5 p. 955 - 958
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 5 p. 992 - 994
反应条件
styrene; n-heptane; sulfuric acid
参考文献
Esso Research and Eng. Co.
Patent: US2730436 , 1952 ;
反应条件
oligomeric (4-methoxyphenyl)alumoxane T=140°C; other ratio of reagents; Product distribution;
参考文献
Inoyatov, F. Kh.; Abubakirov, R. Sh.; Mikaya, A. I.; Khrapova, I. M.; Perchenko, V. M.; Plate, N. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 5 p. 955 - 958
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 5 p. 992 - 994