5-甲基-2-异丙基环己酮合成路线 （共 238 条）
反应条件
diethyl ether; sodium
参考文献
Beckmann
Journal fuer Praktische Chemie (Leipzig), 1897 , vol. <2> 55, p. 17
Chem. Zentralbl., 1887 , vol. 58, p. 1375,1461
反应条件
1: 79.1 percent / Et3N / dimethylformamide / 47 h / 150 °C View Scheme
参考文献
Shono,T. et al.
Tetrahedron Letters, 1974 , p. 1295 - 1298
反应条件
hydrogen in cyclohexane T=120°C; P=22502.3 Torr; 3 h;
参考文献
Pickard; Littlebury
Journal of the Chemical Society, 1912 , vol. 101, p. 116
反应条件
hydrogen; Co-Tart in acetic acid; ethyl acetate T=130°C; P=75005.9 Torr; 13 h; Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 8.2 p. 1765 - 1768
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1920 - 1923
反应条件
hydrogen; Co-Tart in acetic acid; ethyl acetate T=130°C; P=75005.9 Torr; 17 h; other catalysts (Co, Ni, Ni-Tart (modified with RR-(+)-tartaric acid)), other solvents, other reaction times; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 8.2 p. 1765 - 1768
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1920 - 1923
反应条件
Chlorella vulgaris 24 h; Culture medium;
参考文献
Ghasemi, Younes; Mohagheghzadeh, Abdolali; Ostovan, Zahra; Moshavash, Maryam; Rasoul-Amini, Sara; Morowvat, Mohammad Hossein
Chemistry of Natural Compounds, 2010 , vol. 46, # 5 p. 734 - 737
参考文献
Pickard; Littlebury
Journal of the Chemical Society, 1912 , vol. 101, p. 116
参考文献
Pickard; Littlebury
Journal of the Chemical Society, 1912 , vol. 101, p. 116
反应条件
1: pyridine; hydroxylamine hydrochloride / ethanol / 40 h / Inert atmosphere; Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 40 h / 0 °C / Inert atmosphere; Reflux View Scheme
参考文献
Payne, Philippa R.; Bexrud, Jason A.; Leitch, David C.; Schafer, Laurel L.
Canadian Journal of Chemistry, 2011 , vol. 89, # 10 p. 1222 - 1229
反应条件
anschliessend Verseifen der entstandenen Formylderivate mit Salzsaeure; Trennung erfolgt durch Unsetzung mit Salicylaldehyd und Hydrolyse des ausgeschiedenen Salicylidenderivats mit verd. Schwefelsaeure;
参考文献
Read; Robertson
Journal of the Chemical Society, 1927 , p. 2173
