5-甲基-2-异丙基环己酮合成路线 （共 238 条）
反应条件
Verseifen der entstandenen Formylderivate mit Salzsaeure;
参考文献
Read; Robertson; Cook
Journal of the Chemical Society, 1927 , p. 1278
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Tutin; Kipping
Journal of the Chemical Society, 1904 , vol. 85, p. 74
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Read; Robertson
Journal of the Chemical Society, 1926 , p. 2218
Journal of the Chemical Society, 1927 , p. 2171
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Wallach
Justus Liebigs Annalen der Chemie, 1893 , vol. 276, p. 306
Justus Liebigs Annalen der Chemie, 1898 , vol. 300, p. 278
反应条件
hydrogen in cyclohexane T=120°C; P=22502.3 Torr; 3 h;
参考文献
Pickard; Littlebury
Journal of the Chemical Society, 1912 , vol. 101, p. 116
反应条件
hydrogen; Co-Tart in acetic acid; ethyl acetate T=130°C; P=75005.9 Torr; 13 h; Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 8.2 p. 1765 - 1768
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1920 - 1923
反应条件
hydrogen; Co-Tart in acetic acid; ethyl acetate T=130°C; P=75005.9 Torr; 17 h; other catalysts (Co, Ni, Ni-Tart (modified with RR-(+)-tartaric acid)), other solvents, other reaction times; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 8.2 p. 1765 - 1768
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1920 - 1923
参考文献
Pickard; Littlebury
Journal of the Chemical Society, 1912 , vol. 101, p. 116
反应条件
1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / 120 h / 25 °C 2: sulfuric acid; N,N,N,N',N',N'-hexamethyl-butane-1,4-diammonium dimethylsulfate / methanol; water / 50 °C / Electrochemical reduction 3: hydrogenchloride / diethyl ether / 0 °C View Scheme
参考文献
Kulisch, Joern; Nieger, Martin; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 24 p. 5564 - 5567
反应条件
sodium ethanolate in ethanol T=45°C; 40 h;
参考文献
Grossmann; Brauer
Journal fuer Praktische Chemie (Leipzig), 1918 , vol. <2> 98, p. 12
反应条件
Nicotiana tabacum cells in water T=25°C; 96 h; biotransformation;
参考文献
Suga, Takayuki; Hirata, Toshifumi; Hamada, Hiroki; Murakami, Satoru
Phytochemistry (Elsevier), 1988 , vol. 27, # 4 p. 1041 - 1044
反应条件
cultured cells of Nicotiana tabacum further reation times; Product distribution;
参考文献
Suga, Takayuki; Hamada, Hiroki; Hirata, Toshifumi; Izumi, Shunsuke
Chemistry Letters, 1987 , p. 903 - 906
反应条件
T=0°C; es bildet sich ein Gleichgewichtsgemisch mit Produkt 1;
参考文献
Hueckel et al.
Justus Liebigs Annalen der Chemie, 1958 , vol. 616, p. 46,80
