2,3-二甲基-3-丁烯-2-醇合成路线 (共 74 条)
反应条件
methanesulfonic acid in dichloromethane-d2
T=26.5°C; various conc. of methanesulfonic acid in the presence and absence of 3-chlorobenzoic acid, effect of sulfuric acid catalyst; Product distributionMechanism;
参考文献
Zon, A. van; Huis, R.
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 11 p. 425 - 429
反应条件
Diethyloxytriphenylphosphorane
1.) C6D6, 7 d, reflux; 2.) 200 deg C, 15 torr; various solvent, temperature, time; Product distribution;
参考文献
Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 - 5219
反应条件
Cs2,8
T=199.85°C; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Molnar; Beregszaszi; Fudala; Lentz; Nagy; Konya; Kiricsi
Journal of Catalysis, 2001 , vol. 202, # 2 p. 379 - 386
反应条件
copper-graphimet in gas
T=250°C; other catalysts; other temp.; Product distribution;
参考文献
Molnar, Arpad; Mastalir, Agnes; Bartok, Mihaly
Journal of the Chemical Society, Chemical Communications, 1989 , p. 124 - 126
反应条件
2,2'-azo-bisisobutyronitrile; oxygen
T=45°C; P=759.8 Torr; 245 h;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.; Willecke, B.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 682 - 686
反应条件
oxygen
T=60°C; P=759.8 Torr; 9 h;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.; Willecke, B.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 682 - 686
反应条件
O(3P)
T=-42°C; Product distributionMechanism;
参考文献
Tanner; Kandanarachchi; Das; Brausen; Vo; Camaioni; Franz
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4587 - 4593
反应条件
hydrogen iodide
T=84 - 93°C; Product distribution; Further Variations:ReagentsTemperaturesconc. of reagents;
参考文献
De Lezaeta, Monica; Sattar, Wajiha; Svoronos, Paris; Karimi, Sasan; Subramaniam, Gopal
Tetrahedron Letters, 2002 , vol. 43, # 51 p. 9307 - 9309
参考文献
Hatch; Journeay
Journal of the American Chemical Society, 1953 , vol. 75, p. 3712
反应条件
T=369.1 - 459.9°C; P=15 Torr; E(excit); KineticsMechanismThermodynamic data;
参考文献
Flowers, Michael C.; Honeyman, Malcolm R.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1981 , vol. 77, p. 1923 - 1933