methanol; diethyl ether; sodium methylate Hydrieren des Reaktionsprodukts an Palladium/Kohle in Aethanol und Erwaermen des erhaltenen Esters mit aethanol.Kalilauge und anschliessend mit konz.wss.Salzsaeure;
参考文献
Acker; Anderson
Journal of Organic Chemistry, 1959 , vol. 24, p. 1162
McElvain; Burkett
Journal of the American Chemical Society, 1942 , vol. 64, p. 1833
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Barnes; Kundiger; McElvain
Journal of the American Chemical Society, 1940 , vol. 62, p. 1285
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McElvain; Burkett
Patent: US2394195 , 1942 ;
sodium ethanolate in ethanol T=140°C; 9 h; Parr bomb;
参考文献
Seeman, Jeffrey I.; Secor, Henry V.; Chavdarian, Charles G.; Sanders, Edward B.; Bassfield, Ronald L.; Whidby, Jerry F.
Journal of Organic Chemistry, 1981 , vol. 46, # 15 p. 3040 - 3048