1: With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; Mukaiyama aldol addition; 2 h; Inert atmosphere; 2: With water; trifluoroacetic acid in ethanol; dichloromethane Inert atmosphere;
参考文献
Downey, C. Wade; Johnson, Miles W.; Lawrence, Daniel H.; Fleisher, Alan S.; Tracy, Kathryn J.
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5351 - 5354
1: With hydrogen fluoride in dichloromethane 2: With methanol-d1 Title compound not separated from byproducts;
参考文献
Golubev, Nikolai S.; Tolstoy, Peter M.; Smirnov, Sergei N.; Denisov, Gleb S.; Limbach, Hans-Heinrich
Journal of Molecular Structure, 2004 , vol. 700, # 1-3 p. 3 - 12
→
反应条件
in water; acetone T=25°C; Kinetics;
参考文献
Schaller, Heike F.; Tishkov, Alexander A.; Feng, Xinliang; Mayr, Herbert
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 3012 - 3022
Schaller, Heike F.; Tishkov, Alexander A.; Feng, Xinliang; Mayr, Herbert
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 3012 - 3022
in water; acetone T=25°C; Kinetics; Further Variations:Solvents;
参考文献
Schaller, Heike F.; Tishkov, Alexander A.; Feng, Xinliang; Mayr, Herbert
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 3012 - 3022
in acetonitrile T=25°C; Kinetics; Further Variations:Solvents;
参考文献
Schaller, Heike F.; Tishkov, Alexander A.; Feng, Xinliang; Mayr, Herbert
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 3012 - 3022
in acetonitrile T=25°C; Kinetics; Further Variations:Solvents;
参考文献
Schaller, Heike F.; Tishkov, Alexander A.; Feng, Xinliang; Mayr, Herbert
Journal of the American Chemical Society, 2008 , vol. 130, # 10 p. 3012 - 3022
