1-(3,4-二甲氧基苯基)-2-(2-甲氧基苯基)-丙烷-1,3-二醇合成路线 (共 41 条)
反应条件
water; [C4mim]Cl T=150°C; 1 h; Sealed vial;
参考文献
ChemSusChem, , vol. 3, # 9 p. 1078 - 1084
反应条件
oxygen in water T=170°C; 3 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1673 - 1679
反应条件
1: hydrogenchloride / ethanol / 3 h / 60 °C 2: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide; dichloromethane / 20 °C 3: formic acid; [Ir(phenylpyridine(-1H))2(4,4′-di-tert-butyl-2,2′-bipyridine)](PF6); N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 20 °C / |Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 4 p. 1218 - 1221
反应条件
oxygen; anhydrous cobalt diacetate; acetic acid T=170°C; P=25857.4 Torr; 3 h; var. reaction partner systems; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1673 - 1679
反应条件
sodium hydroxide in water T=150 - 160°C; electrochemical oxidation; other conditions: other solvents, other reagents, reaction in the presence of tris(4-bromophenyl)amine as mediator, other temperature, different electrodes; <other lignin model dimers as starting material>; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 56, # 26 p. 7305 - 7313
反应条件
hydrogenchloride; sulfuric acid in 1,4-dioxane; water 4 h; Heatingacid degradation; other acids;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 42, # 1 p. 48 - 51
反应条件
potassium peroxomonosulphate; manganese porphyrin in water; acetonitrile 0.25 h; Ambient temperatureoxidation catalyzed by various supported porphyrins on regular ion-exchange resins or on a poly(vinylpyridinium)polymer; Product distribution;
参考文献
Pattou, Denis; Labat, Gilles; Defrance, Sabine; Seris, Jean-Louis; Meunier, Bernard
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 1 p. 78 - 88
反应条件
[bis(acetoxy)iodo]benzene; oxygen in ethyl acetate T=80°C; P=760.051 Torr; 24 h; chemoselective reaction;
参考文献
Chemical Communications, , vol. 49, # 97 p. 11439 - 11441
反应条件
[bis(acetoxy)iodo]benzene; oxygen T=100°C; P=760.051 Torr; 24 h; Solvent; chemoselective reaction;
参考文献
Chemical Communications, , vol. 49, # 97 p. 11439 - 11441
反应条件
oxygen in water T=170°C; 3 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1673 - 1679