1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in chloroform-d1 (under N2, Schlenk); I2 added to soln. of Pd-complex in CDCl3; evapd., residue extd. with CS2, filtered, evapd.;
参考文献
Dalton Transactions, , vol. 41, # 7 p. 1991 - 2002
反应条件
in neat (no solvent) byproducts: CO2, H2; react. of SO2 and CO in presence of steam studied, formation of S6 and S8 when SO2 excess or temps. below 600°C together with redn. of H2S amount;;
参考文献
Zhurnal khim. Promyshlennosti (russ.), , vol. 8, p. 109 - 119
反应条件
in neat (no solvent) Kinetics; byproducts: S5, S9; Irradiation (UV/VIS); photolysis (high pressure Hg lamp, 200-600 nm) in the presence or absence of air, 15°C; monitoring by HPL chromy.;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 6 p. 682 - 690
反应条件
in neat (no solvent) byproducts: CO2, CO; passing pure SO2 over C, equilibrium composition of resulting gas before deposition of S at 350°C calcd.;;
参考文献
Industrial and Engineering Chemistry, , vol. 30, p. 92 - 100
S: MVol.B1, 122, page 267 - 269
反应条件
in carbon disulfide Kinetics; byproducts: S9, S11, S14; Irradiation (UV/VIS); photolysis (high pressure Hg lamp, 200-600 nm), 15°C; further product: S5 (traces); monitoring by HPL chromy.;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 6 p. 682 - 690
反应条件
in dichloromethane; dichloromethane-d2 further products; NMR-tube; products not isolated; (19)F-, (14)N- and (1)H-NMR spectroscopy;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 571, p. 82 - 90
参考文献
Angewandte Chemie, , vol. 58, p. 52 - 60
反应条件
in gas on the surface of Ti sponge, 300°C; trapped at -196°C, elem. anal., mass spect.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 731 - 735
反应条件
in carbon disulfide react. of Ti-compd. with S2Cl2 in CS2 at 20°C;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 349 - 354
反应条件
in neat (no solvent) thermal decompn., under N2, 140-180°C, Pt-crucible;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 33, p. 1271 - 1272
Zhurnal Neorganicheskoi Khimii, , vol. 33, p. 2225 - 2227
