1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
byproducts: S15, S20;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 349 - 354
反应条件
in methanol Kinetics;
参考文献
Gmelin Handbook: C: MVol.D1, 3.4, page 31 - 44
反应条件
in chloroform-d1 N2 atmosphere, 16 h; not isolated;
参考文献
Noble, Mark E.; Williams, Donald E.
Inorganic Chemistry, 1988 , vol. 27, p. 749 - 752
参考文献
Vyazankin, N. S.; Bochkarev, M. N.; Sanina, L. P.
Zhurnal Obshchei Khimii, 1966 , vol. 36, p. 166 - 166
Full Text Show Details
Vyazankin, N. S.; Bochkarev, M. N.; Sanina, L. P.
Zhurnal Obshchei Khimii, 1966 , vol. 36, p. 1961 - 1964
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.8, page 63 - 65
反应条件
aluminium (N2), bomb reed, refluxed at 160°C for 10 min; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
反应条件
(N2), bomb reed, heated at 245°C for 66 h; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
反应条件
in neat (no solvent) dry box; dissolving S in Se2Cl2 by heating several min; further products; not isolated; detn. by Raman- and (77)Se-NMR spectroscopy;
参考文献
Milne, John B.
Canadian Journal of Chemistry, 1992 , vol. 70, # 3 p. 693 - 699
反应条件
NH3 in ammonia NH3 (liquid); inert atmosphere;
参考文献
O'Mahoney, Caroline A.; Parkin, Ivan P.; Williams, David J.; Woollins, J. Derek
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1179 - 1186
反应条件
1: sulfur; cyanoacetic acid ethyl ester With triethylamine in N,N-dimethyl-formamide T=20°C; 0.166667 h; 2: butyraldehyde in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
DEVELOGEN AKTIENGESELLSCHAFT
Patent: WO2006/136402 A1, 2006 ;
Location in patent: Page/Page column 79 ;
WO 2006/136402 A1
反应条件
in not given sublimation in a high-vac.;;
参考文献
Preuss, Fritz; Noichl, Harald
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 2 p. 121 - 129
