1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in neat (no solvent) isocyanate condensation onto borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
反应条件
in neat (no solvent) isocyanate condensation onto borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
反应条件
in neat (no solvent) isocyanate condensation onto solid borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
反应条件
in benzene byproducts: Cu2Cl2, CO; 80°C, 8 h; filtn., washing ppt. (hot benzene), chromy. of filtrate after removing solvent;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 56, p. 1624 - 1627
Zhurnal Obshchei Khimii, , vol. 56, p. 1837 - 1840
反应条件
in carbon disulfide Ar; S-compd. soln. addn. dropwise to Se-compd. soln. at -78°C, mixt. allowing to warm slowly to room temp. (stirring, 12 h); elem. anal., (77)Se-NMR;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 124, p. 457 - 460
反应条件
in tetrahydrofuran; water aq. hydroxylamine dissolved in THF, treated dropwise with 1-2 equiv. of CS2 at ice temp., warmed to room temp. over 45 min, stirred at room temp. for 3 h (mechanism discussed); ppt. filtered, kept at 7°C for 4 d, pptd., washed (ethyl acetate), dried (vac.);
参考文献
Inorganic Chemistry Communications, , vol. 13, # 5 p. 622 - 624
反应条件
carbon monoxide; platinum byproducts: CO2, COS; in CO atmosphere, at 400°C; react. accelerated by Pt, Ni-Cu catalysts;
参考文献
Silikattechnik, , vol. 2, p. 172 - 176
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 264, p. 272 - 284
反应条件
in neat (no solvent) isocyanate condensation onto borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.);
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
反应条件
in neat (no solvent) isocyanate condensation onto borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
反应条件
in neat (no solvent) isocyanate condensation onto borole (N2, -196°C), slow warming to room temp., heating (120°C, 14 h); distn. (high vac.); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. 289 - 298
